{"id":105,"date":"2012-04-23T19:00:46","date_gmt":"2012-04-23T19:00:46","guid":{"rendered":"http:\/\/innovscience.com\/wordpress\/?p=105"},"modified":"2012-04-23T19:01:04","modified_gmt":"2012-04-23T19:01:04","slug":"story-of-the-goat-man-part-6","status":"publish","type":"post","link":"https:\/\/innovscience.com\/wordpress\/uncategorized\/story-of-the-goat-man-part-6\/","title":{"rendered":"Story of the Goat Man (Part 6)"},"content":{"rendered":"<p><a href=\"http:\/\/innovscience.com\/wordpress\/wp-content\/uploads\/2012\/04\/dry-box-window-frament-and-wire.jpg\"><img loading=\"lazy\" decoding=\"async\" class=\"alignnone size-medium wp-image-106\" title=\"dry box window frament and wire\" src=\"http:\/\/innovscience.com\/wordpress\/wp-content\/uploads\/2012\/04\/dry-box-window-frament-and-wire-300x225.jpg\" alt=\"\" width=\"300\" height=\"225\" srcset=\"https:\/\/innovscience.com\/wordpress\/wp-content\/uploads\/2012\/04\/dry-box-window-frament-and-wire-300x225.jpg 300w, https:\/\/innovscience.com\/wordpress\/wp-content\/uploads\/2012\/04\/dry-box-window-frament-and-wire-1024x768.jpg 1024w, https:\/\/innovscience.com\/wordpress\/wp-content\/uploads\/2012\/04\/dry-box-window-frament-and-wire-400x300.jpg 400w, https:\/\/innovscience.com\/wordpress\/wp-content\/uploads\/2012\/04\/dry-box-window-frament-and-wire.jpg 2048w\" sizes=\"(max-width: 300px) 100vw, 300px\" \/><\/a><\/p>\n<p>It was now around this time that Sam came close to dying.\u00a0 While attempting to repeat one of Smirnov\u2019s experiments a serious explosion occurred inside the glove box Sam was working in.\u00a0 This explosion entirely blew out the back window hurling its pieces (above) a good 40 feet.\u00a0 It flexed the front window up against Sam\u2019s face and pushed his hands immediately out forcing him back several feet.\u00a0 A roll of paper towels inside caught on fire and Sam fortunately had enough composure to put that out with a fire extinguisher as the box had a cooling well in it already filled with about 4-5 gallons of heptane (i.e. gasoline).\u00a0 Had the front window broke Sam would have been decapitated.\u00a0 The University of Asscrack never supplied Sam with any official paperwork to fill out although he did supply them with a lengthy handwritten testimony of the accident.\u00a0 They never disclosed the actual cause of the accident to him or provided any photographs and according to the memo affixed (below) with his testimony (below) the explosion (according to University of Asscrack offals, yes no misspelling) was minor.\u00a0 Instead they hushed it up quickly.\u00a0 Sam told me that he thinks there is a possibility it could have been arranged to happen (i.e. kill Sam) as he later found an unusual wire (above) that may have come from an electric motor used inside the box.\u00a0 Despite these boxes having supposedly been under an inert atmosphere he knew they contained enough moisture to cause metal halides (being withdrawn via syringe from a septum sealed bottle mind you) to fume so profusely as to obscure the view through the box itself.\u00a0 So the oxygen level may have even been quite high as well.\u00a0 He also knew that the stirring motor for the cooling bath occasionally had an electrical glow to it but was told by others of the herd that it was an indication that no oxygen or moisture were present.\u00a0 In his usual 20\/20 hindsight Sam said use of electric devices in such a piece of equipment (that were not explosion proof) would have been an obvious safety violation.\u00a0 Moreover, Sam told me that these boxes routinely contained mL (e.g. + 10 mL) quantities of isobutene and sometimes methyl chloride that would eject from immersion cooling coils used for their collection inside the box.\u00a0 On rereading his account of the accident Sam mentioned to me that the box may have been precharged with isobutene or methyl chloride as the valves for the latter gas we in the open position prior to experimentation, which was unusual.\u00a0 These materials due to their volatility and flammability would be an ideal explosive under the right conditions.\u00a0 Regardless of the cause, planned or not it was a turning point for Sam.<\/p>\n<p><a href=\"http:\/\/innovscience.com\/wordpress\/wp-content\/uploads\/2012\/04\/Memo-names-blocked.jpg\"><img loading=\"lazy\" decoding=\"async\" class=\"alignnone size-medium wp-image-107\" title=\"Memo names blocked\" src=\"http:\/\/innovscience.com\/wordpress\/wp-content\/uploads\/2012\/04\/Memo-names-blocked-218x300.jpg\" alt=\"\" width=\"218\" height=\"300\" srcset=\"https:\/\/innovscience.com\/wordpress\/wp-content\/uploads\/2012\/04\/Memo-names-blocked-218x300.jpg 218w, https:\/\/innovscience.com\/wordpress\/wp-content\/uploads\/2012\/04\/Memo-names-blocked-744x1024.jpg 744w\" sizes=\"(max-width: 218px) 100vw, 218px\" \/><\/a><\/p>\n<p><a href=\"http:\/\/innovscience.com\/wordpress\/wp-content\/uploads\/2012\/04\/Page-1-of-account-names-blocked.jpg\"><img loading=\"lazy\" decoding=\"async\" class=\"alignnone size-medium wp-image-108\" title=\"Page #1 of account names blocked\" src=\"http:\/\/innovscience.com\/wordpress\/wp-content\/uploads\/2012\/04\/Page-1-of-account-names-blocked-218x300.jpg\" alt=\"\" width=\"218\" height=\"300\" srcset=\"https:\/\/innovscience.com\/wordpress\/wp-content\/uploads\/2012\/04\/Page-1-of-account-names-blocked-218x300.jpg 218w, https:\/\/innovscience.com\/wordpress\/wp-content\/uploads\/2012\/04\/Page-1-of-account-names-blocked-744x1024.jpg 744w\" sizes=\"(max-width: 218px) 100vw, 218px\" \/><\/a><\/p>\n<p><a href=\"http:\/\/innovscience.com\/wordpress\/wp-content\/uploads\/2012\/04\/Page-2-of-Account.jpg\"><img loading=\"lazy\" decoding=\"async\" class=\"alignnone size-medium wp-image-109\" title=\"Page #2 of Account\" src=\"http:\/\/innovscience.com\/wordpress\/wp-content\/uploads\/2012\/04\/Page-2-of-Account-218x300.jpg\" alt=\"\" width=\"218\" height=\"300\" srcset=\"https:\/\/innovscience.com\/wordpress\/wp-content\/uploads\/2012\/04\/Page-2-of-Account-218x300.jpg 218w, https:\/\/innovscience.com\/wordpress\/wp-content\/uploads\/2012\/04\/Page-2-of-Account-744x1024.jpg 744w\" sizes=\"(max-width: 218px) 100vw, 218px\" \/><\/a><\/p>\n","protected":false},"excerpt":{"rendered":"<p>It was now around this time that Sam came close to dying.\u00a0 While attempting to repeat one of Smirnov\u2019s experiments a serious explosion occurred inside the glove box Sam was working in.\u00a0 This explosion entirely blew out the back window &hellip; <a href=\"https:\/\/innovscience.com\/wordpress\/uncategorized\/story-of-the-goat-man-part-6\/\">Continue reading <span class=\"meta-nav\">&rarr;<\/span><\/a><\/p>\n","protected":false},"author":1,"featured_media":0,"comment_status":"open","ping_status":"open","sticky":false,"template":"","format":"standard","meta":{"_jetpack_newsletter_access":"","_jetpack_dont_email_post_to_subs":false,"_jetpack_newsletter_tier_id":0,"_jetpack_memberships_contains_paywalled_content":false,"_jetpack_memberships_contains_paid_content":false,"footnotes":""},"categories":[1],"tags":[],"jetpack_featured_media_url":"","jetpack_sharing_enabled":true,"jetpack_shortlink":"https:\/\/wp.me\/pb8bvA-1H","_links":{"self":[{"href":"https:\/\/innovscience.com\/wordpress\/wp-json\/wp\/v2\/posts\/105"}],"collection":[{"href":"https:\/\/innovscience.com\/wordpress\/wp-json\/wp\/v2\/posts"}],"about":[{"href":"https:\/\/innovscience.com\/wordpress\/wp-json\/wp\/v2\/types\/post"}],"author":[{"embeddable":true,"href":"https:\/\/innovscience.com\/wordpress\/wp-json\/wp\/v2\/users\/1"}],"replies":[{"embeddable":true,"href":"https:\/\/innovscience.com\/wordpress\/wp-json\/wp\/v2\/comments?post=105"}],"version-history":[{"count":3,"href":"https:\/\/innovscience.com\/wordpress\/wp-json\/wp\/v2\/posts\/105\/revisions"}],"predecessor-version":[{"id":112,"href":"https:\/\/innovscience.com\/wordpress\/wp-json\/wp\/v2\/posts\/105\/revisions\/112"}],"wp:attachment":[{"href":"https:\/\/innovscience.com\/wordpress\/wp-json\/wp\/v2\/media?parent=105"}],"wp:term":[{"taxonomy":"category","embeddable":true,"href":"https:\/\/innovscience.com\/wordpress\/wp-json\/wp\/v2\/categories?post=105"},{"taxonomy":"post_tag","embeddable":true,"href":"https:\/\/innovscience.com\/wordpress\/wp-json\/wp\/v2\/tags?post=105"}],"curies":[{"name":"wp","href":"https:\/\/api.w.org\/{rel}","templated":true}]}}